Spectrometric Identification of Organic Compounds
Average customer rating: 3.5 out of 5 stars
  • Excellent excercises...
  • Reference vs. Teaching Material
  • Great material, regular text...
  • An Important book
  • Good in NMR Spectra analysis information, but weak elsewhere
Spectrometric Identification of Organic Compounds
Robert M. Silverstein , Francis X. Webster , and David Kiemle
Manufacturer: Wiley
ProductGroup: Book
Binding: Hardcover

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ASIN: 0471393622

Book Description

Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:

Customer Reviews:

4 out of 5 stars Excellent excercises..........2006-03-12

It's an OK book if you are a novice in the Spectroscopy determination area, but a very nice book if it's going to be used as a reference book. It's very handy and explains the principles of the Spectroscopic and Spectrometric determinations in a very understandable way. Moreover, the excercises are challenging, making this book and excellent tool for those students interested in learning how to determine structures out of some spectra, although the spectra sometimes are so clean that they don't correspond with the one's that are taken by routine. The weak points of this book are the IR chapter and the lack of a UV chapter explaining various useful techniques for structural determination such as ORD and CD. The NMR section is just OK, but there are more details to be explained in the 2-D NMR NOESY, TOCSY and ROESY. I think the Mass Chapters are the best that any single book has offered to me so far to understand quite easily how powerful is the GCMS as a tool for the Structural Determination of Organic Compounds.

3 out of 5 stars Reference vs. Teaching Material.......2005-03-05

This book has wonderful charts and tables for quick referencing, however it is sorely lacking in demonstrations and worked out examples for students new to the subject. The chapters are painfully slow and complex when explaining the theory behind the spectrometric methods and effects on classes of molecules. In short, don't use this book to learn the material unless you already know it. It is a comprehensive reference, but not an effective textbook to teach from.

3 out of 5 stars Great material, regular text..........2001-07-17

The book is subdivided into only 3 of the 4 classical methods for spectrometric identification of compounds: IR, MS, and finally NMR (covering 1H, 13C and very little of 19F and 31P). UV is left out in this edition, so maybe getting a hold of the old edition's UV chapter (which is extremely well-written) might be desired. The MS and the IR chapters are also well-written and explained out. It is in the main technique (NMR) that the author fails to deliver the subject in a straightforward manner and lacks what I think is most important in this field: a large number of exercises and problems.

5 out of 5 stars An Important book.......2000-05-10

This book provide a the basis of the fundamentals of Spectroscopy in many fields (IR, HNMR, CNMR, DEPT, COSY, HMBC, HMQC, TOCSY, MS, and much more) It has many real problems in an special chapter. And the most important, it has a lot of important tables and spectrums.

3 out of 5 stars Good in NMR Spectra analysis information, but weak elsewhere.......1999-11-19

This book lacked information in my opinion. Silverstein started a good project but just didn't give enough information about IR interpretation, mass spec, C-13 NMR, etc. He focussed on 2-D NMR a great deal, and I believe that there are much better textbooks on this subject.
Applications of Mass Spectrometry to Organic Sterochemistry (Methods in Stereochemical Analysis)
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    Applications of Mass Spectrometry to Organic Sterochemistry (Methods in Stereochemical Analysis)

    Manufacturer: Wiley-VCH
    ProductGroup: Book
    Binding: Hardcover

    General & ReferenceGeneral & Reference | Chemistry | Science | Subjects | Books
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    ASIN: 0471186767

    Book Description

    Packed with reviews plus new results from the author's laboratories, the first-of-its-kind work offers a timely and authoritative treatise on the use of mass spectral techniques in organic stereochemistry.

    Featuring 22 chapters contributed by eminent and active researchers in the field, this unique sourcebook offers comparative information on the use of a variety of mass-spectral techniques to characterize stereoisomers and conformers of both large and small biologically important organic molecules. It also discusses techniques for studying gas-phase conformational equilibria in conformationally mobil systems.

    Applications of Mass Spectrometry to Organic Stereochemistry will dramatically aid the lab applications of organic, biological, pharmaceutical, and analytical chemists in university and industrial laboratories.
    Infrared Spectra of Inorganic Compounds (3800-45cm-1)
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      Infrared Spectra of Inorganic Compounds (3800-45cm-1)

      Manufacturer: Academic Press
      ProductGroup: Book
      Binding: Hardcover

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      ASIN: 0125234503
      Ion Formation from Organic Solids (Ifos IV : Mass Spectrometry of Involatile Material : Proceedings of the Fourth International Conference, Munster,)
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        Ion Formation from Organic Solids (Ifos IV : Mass Spectrometry of Involatile Material : Proceedings of the Fourth International Conference, Munster,)

        Manufacturer: John Wiley & Sons Inc
        ProductGroup: Book
        Binding: Hardcover

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        ASIN: 0471924857
        IONIZATION METHODS IN ORGANIC (RSC Analytical Spectroscopy Monographs)
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          IONIZATION METHODS IN ORGANIC (RSC Analytical Spectroscopy Monographs)
          A ASHCROFT
          Manufacturer: Royal Society of Chemistry
          ProductGroup: Book
          Binding: Hardcover

          AnalyticAnalytic | Chemistry | Science | Subjects | Books
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          ASIN: 0854045708
          Mass Spectrometry of Heterocyclic Compounds (General heterocyclic chemistry series)
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            Mass Spectrometry of Heterocyclic Compounds (General heterocyclic chemistry series)
            Q.N. Porter , and J. Baldas
            Manufacturer: John Wiley & Sons Inc
            ProductGroup: Book
            Binding: Hardcover

            General & ReferenceGeneral & Reference | Chemistry | Science | Subjects | Books
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            ASIN: 0471695041
            Mass Spectrometry of Organic Compounds
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              Mass Spectrometry of Organic Compounds
              Herbert. Budzikiewicz
              Manufacturer: Holden Day
              ProductGroup: Book
              Binding: Textbook Binding
              ASIN: 0816212112
              Practical Organic Mass Spectrometry: A Guide for Chemical and Biochemical Analysis
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                Practical Organic Mass Spectrometry: A Guide for Chemical and Biochemical Analysis
                J. R. Chapman
                Manufacturer: John Wiley & Sons Inc
                ProductGroup: Book
                Binding: Hardcover

                GeneralGeneral | Science | Subjects | Books
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                Atomic & Nuclear PhysicsAtomic & Nuclear Physics | Nuclear Physics | Physics | Science | Subjects | Books
                Mass SpectrometryMass Spectrometry | Spectroscopy | Chemistry | Science | Subjects | Books
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                ASIN: 0471927538

                Book Description

                Practical Organic Mass Spectrometry Second Edition A Guide for Chemical and Biochemical Analysis J. R. Chapman Kratos Analytical Instruments, Manchester, UK This volume provides a comprehensive survey of current techniques for the use of mass spectrometry in organic chemical and biochemical analysis. Every aspect of modern instrumentation and technique is discussed. The new edition retains the effective division of material applied in the author's previous volume-theory, practical requirements and applications. However, it has been thoroughly revised and extended to include all recent advances in mass spectrometry, and is complete with extensive references. This is essentially a book for the practising mass spectroscopist which will appeal to both biochemists and organic chemists. Some familiarity with basic principles is assumed but the author has employed a style which makes this volume suitable for beginners and more advanced students alike. The present volume will be particularly valuable to anyone who wishes to evaluate and compare alternative techniques. Main Contents-Instrumentation; Sample Introduction; Chemical lonization (lon-Molecule Reactions); Negative lon Chemical lonization; The lonization of Labile Materials (Part I); The lonization of Labile Materials (Part II); Tandem Mass Spectrometry (The Dissociation of lons); Quantitative Analysis.
                Chemical analyses of organic residues in archaeological pottery from Arbon Bleiche 3, Switzerland - evidence for dairying in the late Neolithic [An article from: Journal of Archaeological Science]
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                  Chemical analyses of organic residues in archaeological pottery from Arbon Bleiche 3, Switzerland - evidence for dairying in the late Neolithic [An article from: Journal of Archaeological Science]
                  J.E. Spangenberg , S. Jacomet , and J. Schibler
                  Manufacturer: Elsevier
                  ProductGroup: Book
                  Binding: Digital

                  ElsevierElsevier | By Publisher | e-Docs | Formats | Books
                  ASIN: B000RR7SI8

                  Book Description

                  This digital document is a journal article from Journal of Archaeological Science, published by Elsevier in . The article is delivered in HTML format and is available in your Amazon.com Media Library immediately after purchase. You can view it with any web browser.

                  Description:
                  Fatty acids distribution and stable isotope ratios (bulk @d^1^3C, @d^1^5N and @d^1^3C of individual fatty acids) of organic residues from 30 potsherds have been used to get further insights into the diet at the Late Neolithic (3384-3370 BC) site of Arbon Bleiche 3, Switzerland. The results are compared with modern equivalents of animal and vegetable fats, which may have been consumed in a mixed ecology community having agrarian, breeding, shepherd, gathering, hunting, and fishing activities. The used combined chemical and isotopic approach provides valuable information to complement archaeological indirect evidence about the dietary trends obtained from the analysis of faunal and plant remains. The small variations of the @d^1^3C and @d^1^5N values within the range expected for degraded animal and plant tissues, is consistent with the archaeological evidence of animals, whose subsistence was mainly based on C"3 plants. The overall fatty acid composition and the stable carbon isotopic compositions of palmitic, stearic and oleic acids of the organic residues indicate that the studied Arbon Bleiche 3 sherds contain fat residues of plant and animal origin, most likely ruminant (bovine and ovine). In several vessels the presence of milk residues provides direct evidence for dairying during the late Neolithic in central Europe.
                  @d^1^3C of volatile organic compounds (VOCS) in airborne samples by thermal desorption-gas chromatography-isotope ratio-mass spectrometry (TD-GC-IR-MS) [An article from: Atmospheric Environment]
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                    @d^1^3C of volatile organic compounds (VOCS) in airborne samples by thermal desorption-gas chromatography-isotope ratio-mass spectrometry (TD-GC-IR-MS) [An article from: Atmospheric Environment]
                    N. Turner , M. Jones , K. Grice , D. Dawson , and Ioppolo-
                    Manufacturer: Elsevier
                    ProductGroup: Book
                    Binding: Digital

                    ElsevierElsevier | By Publisher | e-Docs | Formats | Books
                    ASIN: B000RR940I

                    Book Description

                    This digital document is a journal article from Atmospheric Environment, published by Elsevier in 2006. The article is delivered in HTML format and is available in your Amazon.com Media Library immediately after purchase. You can view it with any web browser.

                    Description:
                    This paper is a preliminary investigation into the use of a thermal desorption-gas chromatography-isotope ratio mass spectrometry (TD-GC-IR-MS) method to determine stable carbon isotopic compositions (@d^1^3C) of low molecular-weight volatile organic compounds (VOCs) in airborne samples (e.g. industrial and car exhaust emissions) as a means of differentiating their sources in the environment. A TD-GC-IR-MS method for obtaining @d^1^3C of VOCs (benzene, toluene, chlorobenzene, ethylbenzene, m-xylene and propylbenzene) in air samples has been optimised, and is proven to be both reproducible and linear. The @d^1^3C of the VOC standards was found to be comparable (within analytical error) to that obtained from direct GC-IR-MS analysis. This novel method of VOC analysis is valuable in environmental and forensic investigations.

                    Industry under pressure: what architects need to know about UBC 7-2.(positive pressure fire testing standard for doors): An article from: Doors and Hardware
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                      Industry under pressure: what architects need to know about UBC 7-2.(positive pressure fire testing standard for doors): An article from: Doors and Hardware
                      Tom Janicak
                      Manufacturer: Door and Hardware Institute
                      ProductGroup: Book
                      Binding: Digital

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                      ASIN: B00098LV2Y
                      Release Date: 2005-07-28

                      Book Description

                      This digital document is an article from Doors and Hardware, published by Door and Hardware Institute on February 1, 1999. The length of the article is 1618 words. The page length shown above is based on a typical 300-word page. The article is delivered in HTML format and is available in your Amazon.com Digital Locker immediately after purchase. You can view it with any web browser.

                      Citation Details
                      Title: Industry under pressure: what architects need to know about UBC 7-2.(positive pressure fire testing standard for doors)
                      Author: Tom Janicak
                      Publication: Doors and Hardware (Magazine/Journal)
                      Date: February 1, 1999
                      Publisher: Door and Hardware Institute
                      Volume: 63 Issue: 2 Page: 24(4)

                      Distributed by Thomson Gale
                      Positive About Inspection
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                        Positive About Inspection
                        Paul Nash
                        Manufacturer: Gower Pub Co
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                        Binding: Paperback

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                        ASIN: 0566083167

                        First with the Most: Nathan Bedford Forrest
                        Average customer rating: 5 out of 5 stars
                        • First with the Most biography
                        First with the Most: Nathan Bedford Forrest
                        Robert Selph Henry
                        Manufacturer: Alpine Fine Arts Collection (UK)
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                        Binding: Hardcover

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                        Similar Items:
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                        4. May I Quote You, General Forrest: Observations and Utterances of the South's Great Generals (May I Quote You--?,) May I Quote You, General Forrest: Observations and Utterances of the South's Great Generals (May I Quote You--?,)
                        5. Nathan Bedford Forrest's Escort And Staff Nathan Bedford Forrest's Escort And Staff

                        ASIN: 0914427725

                        Customer Reviews:

                        5 out of 5 stars First with the Most biography.......2006-10-05

                        Alright, I admit it, what first interested me in this particular version was the price. I found it on the discount rack at a bookstore and started reading that night. I found it difficult to put down and finished quickly. It was the first biography of Forrest I had read (some years ago) and I was pleasently surprised to find that he was not demonized but judged in the context of his time. Good biography should do just that - keep the person in the context of their time. Mr. Henry's volume may remain my favorite biography of this brilliant general. There are other good ones but it is always difficult to better your first love.
                        First With the Most :Forrest
                        Average customer rating: Not rated
                          First With the Most :Forrest
                          Robert S Henry
                          Manufacturer: BOBBS MERRILL CO
                          ProductGroup: Book
                          Binding: Hardcover
                          ASIN: B000PY0S62
                          First With the Most Forrest
                          Average customer rating: 4.5 out of 5 stars
                          • A Great Work
                          • Excellent concentration on Forrest's campaigns
                          • A good read...
                          First With the Most Forrest
                          Robert Selph Henry
                          Manufacturer: Broadfoot Pub Co
                          ProductGroup: Book
                          Binding: Hardcover
                          ASIN: 0916107221

                          Customer Reviews:

                          5 out of 5 stars A Great Work.......2004-12-04

                          Forrest, though contreversial was without a doubt one of the best generals on either side in the Civil War. He was able to do more with less than many others in similar situations. With no education and being looked down upon by most of his peirs that is an especially impressive achievement.

                          Henry's work is also good in that it allows us to contrast biographies todaywith the ones from previous times. Henry pays little attention to Foresst's role in the Klan and portrays his slave trading and slave holding in the most positive light possible (dim though that may be). A more modern biographer might well blaze a blinding light upon these activities to the exclusion of his battlefield achievements.

                          I would recomend this work to the reader interested in the Civil War. It does not cover much else in the life of Forrest. It is well written and a good read.

                          5 out of 5 stars Excellent concentration on Forrest's campaigns.......2003-02-21

                          Forrest was an amazing man, a complex man, before, during and after the Civil War. Men despised him because he was so bloody effective, but those same men were forced to grudging respect of Forrest's brilliance. This is not a balanced view of his life, but an excellent concentration of his campaigns. I would suggest reading Jack Hurst's work and John Allan Wyeth's in connection to this book. I have seen some grump because Hurst did not have maps and military information in his book. This will give them all the information they need.

                          Henry work is essential to understanding the whole, but the other two works should be utilised in conjunction to obtain a fully understanding. I cannot recommend them enough for someone starting in the search for a man that is so amazing.

                          4 out of 5 stars A good read..........1999-08-12

                          This is a biography of one of the most misunderstood leaders of the Second War for American Independence, Lt. Gen. N. B. Forrest, CSA. While concentrating on the war years, Henry does give light into Forrest's postwar activity, including his official disbanding of the KKK in 1868, a fact generally overlooked by yankee revisionist historians. A good read, and reccommended.
                          "First With the Most" Forrest
                          Average customer rating: Not rated
                            "First With the Most" Forrest

                            Manufacturer: The Bobbs-Merrill Company
                            ProductGroup: Book
                            Binding: Hardcover
                            ASIN: B000EVG7SO
                            "First with the Most" Forrest
                            Average customer rating: Not rated
                              "First with the Most" Forrest
                              Robert Selph Henry
                              Manufacturer: Bobbs-Merrill Company
                              ProductGroup: Book
                              Binding: Hardcover
                              ASIN: B000O7MYAI
                              First with the Most: Forrest. [Biography of Nathan Bedford Forrest].
                              Average customer rating: Not rated
                                First with the Most: Forrest. [Biography of Nathan Bedford Forrest].
                                Robert Selph. Henry
                                Manufacturer: Konecky & Konecky c
                                ProductGroup: Book
                                Binding: Hardcover
                                ASIN: B000KIV6HS
                                First With the Most: Nathan Bedford Forrest
                                Average customer rating: 4.5 out of 5 stars
                                • A+
                                • Very in depth though weak in areas...
                                • This is one of the best histories of Forrest
                                First With the Most: Nathan Bedford Forrest
                                Robert Selph Henry
                                Manufacturer: BDD Promotional Books Company
                                ProductGroup: Book
                                Binding: Hardcover

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                                Customer Reviews:

                                5 out of 5 stars A+.......2007-01-14

                                A great book. NBF was the real deal. You will enjoy this one.

                                Long Live the South!!! yeeeee hhhaaaaaa

                                3 out of 5 stars Very in depth though weak in areas..........2002-09-30

                                This is one of those books that certainly captures the military career of Nathan Bedford Forrest without getting into much of his personal life history. For trying to understand the man I would suggest Hursts' biography on Forrest. This book was a rather in depth study of every situation Forrest was in during the Civil War. It is strictly military and though thorough, it's lack of maps was troubling. The maps used in the book rarely define the movements or are complicated to understand and poorly demonstrated. Often they are used for a multiple of operations and are completely vague. Had they been better implemented with information and used more often it would have truly completed this book. I found this book by Henry to be less detailed in more popular matters of surrender and enemy deception compared to other books on Forrest. It was easy to get lost at times in regards to reading about generals under Forrest and their movements throughout the western campaign. Is this the best book on Forrest? Military speaking I rank it high, though as a well rounded biography it certainly isn't one as I don't think the author intended to bring that part of the man forward. This book I found boring at times and I wondered how 465 of pages could be filled when detail about the man never surfaced except trivial military matters.

                                5 out of 5 stars This is one of the best histories of Forrest.......2002-01-18

                                This is the standard for Nathan Bedford Forrest history. One of the most brilliant generals of all time. This book really gets into his campaigns and life. Great book and must read for any Civil War history buff; especially one from Tennessee.
                                "First with the Most" Forrest.
                                Average customer rating: Not rated
                                  "First with the Most" Forrest.
                                  Robert Selph. Henry
                                  Manufacturer: Broadfoot Publishing Company
                                  ProductGroup: Book
                                  Binding: Hardcover
                                  ASIN: B000OD04NQ
                                  First With the Most :Forrest
                                  Average customer rating: Not rated
                                    First With the Most :Forrest
                                    Robert S Henry
                                    Manufacturer: BOBBS MERRILL CO
                                    ProductGroup: Book
                                    Binding: Hardcover
                                    ASIN: B000N7CCDS
                                    FIRST WITH THE MOST FORREST
                                    Average customer rating: Not rated
                                      FIRST WITH THE MOST FORREST
                                      Nathan Bedford. Robert Henry Forrest
                                      Manufacturer: Konecky & Konecky
                                      ProductGroup: Book
                                      Binding: Hardcover
                                      ASIN: B000RAVHVO

                                      Fibromyalgia: You Are Not Crazy
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                                        Fibromyalgia: You Are Not Crazy
                                        Dawn Smith
                                        Manufacturer: Trafford Publishing
                                        ProductGroup: Book
                                        Binding: Paperback

                                        GeneralGeneral | Biographies & Memoirs | Subjects | Books
                                        MedicalMedical | Professionals & Academics | Biographies & Memoirs | Subjects | Books
                                        ASIN: 1553958179
                                        Release Date: 2006-07-06

                                        Book Description



                                        As a book I would recommend, Doctors know no one can better describe their symptoms than the patient can themselves. Dawn Smith has done a wonderful job of opening the door of the mysteries of the disease Fibromyalgia and Chronic Fatigue Syndrome.

                                        Having and continuing to live with both diseases, adding her perseverance and contact with others experiencing the same makes this book unique for the reader.

                                        Now retired nurse, Dawn has created this book without medical terms or dry reading and replaced it with life experiences to be expected. Well written. Guaranteed to hold your attention.

                                        Michael J. Armentrout, M.D.
                                        You're Not Crazy! An Overcomers Guide to Fibromyalgia
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                                          You're Not Crazy! An Overcomers Guide to Fibromyalgia
                                          Timothy Weir D.C.
                                          Manufacturer: Lulu.com
                                          ProductGroup: Book
                                          Binding: Paperback

                                          Family HealthFamily Health | Parenting & Families | Subjects | Books
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                                          ASIN: 1430313471

                                          Book Description

                                          This easy to read book written by Dr. Tim Weir, has been updated with the latest research on Fibromyalgia. This dreaded disease has plagued millions, and now he gives common sense solutions to some severe problems. Give this book to someone that you know suffers from muscle aches, headaches, depression. This book will give them hope for the future!

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